Synthesis and Characterization of Methyl Amino Polystyrene as Resin Material of Chromatography

Journal of Tropical Pharmacy and Chemistry

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Field Value
 
Title Synthesis and Characterization of Methyl Amino Polystyrene as Resin Material of Chromatography
 
Creator Herman, Herman
Anggraeni, Anni
Mutalib, Abdul
Bahti, Husein H.
 
Description Ion-exchange chromatography has been widely used in various separation process and purification. Commercial ion-exchange resin mostly uses polystyrene as stationer phase. This study reviewed the synthesis of cation-exchange resin with polystyrene as starting material. Polystyrene must be activated in order to make one of aromatic carbon chains being able to be binding with acetamide n-hidroxymethyl electrophilic. Polystyrene activation was conducted through two stages, i.e. (1) the formation of amidomethyl polystyrene (AMDP), and followed with (2) elimination of acyl group. The activation of polystyrene generated white methylamino polystyrene (MAP) resin, of which its characterization used spectrophotometry UV, Fourier Transform-Infrared (FTIR), and density of MAP resin confirmed by pycnometer. The results showed that the characterization of FTIR and spectrophotometer UV for AMP exhibited forming amino propyl group at 3374.52 cm-1 with λmax 230 nm due to N–H bond; and the average of density of AMP resin sample was 1.7158 g/mL.
 
Publisher Faculty of Pharmacy, Universitas Mulawarman, Samarinda, Indonesia, 75117
 
Date 2019-01-18
 
Type info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
Peer-reviewed Article
 
Format application/pdf
 
Identifier https://jtpc.farmasi.unmul.ac.id/index.php/jtpc/article/view/204
10.25026/jtpc.v4i4.204
 
Source Journal of Tropical Pharmacy and Chemistry; Vol 4 No 4 (2018): Journal of Tropical Pharmacy and Chemistry; 194-201
2407-6090
2087-7099
10.25026/jtpc.v4i4
 
Language eng
 
Relation https://jtpc.farmasi.unmul.ac.id/index.php/jtpc/article/view/204/174
 
Rights Copyright (c) 2018 Journal of Tropical Pharmacy and Chemistry
http://creativecommons.org/licenses/by-nc/4.0
 

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