Growth, optical, spectral, thermal and mechanical investigations of organic NLO crystal cis-2, 6-bis(4-chlorophenyl)-3, 3-dimethylpiperidin-4-one

Bulletin of Scientific Research

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Title Growth, optical, spectral, thermal and mechanical investigations of organic NLO crystal cis-2, 6-bis(4-chlorophenyl)-3, 3-dimethylpiperidin-4-one
 
Creator V, Mohanraj
S.S., Ilango
S, Ponnuswamy
 
Subject Crystal growth
Solubility
Microhardness
Thermal properties
 
Description The single crystal of cis-2,6-bis(4-chlorophenyl)-3,3-dimethylpiperidin-4-one (4C3DMPO) has been grown using a slow evaporation technique. 4C3DMPO is a non-centrosymmetric crystal which crystallizes in the orthorhombic system with space group Pna21. Benzene is used as a solvent for the crystal growth based on solubility studies. The mechanical studies, using microhardness methods, have also been carried out. The compound is characterised using UV, FT-IR and NMR spectral studies. Furthermore, the thermal stability of the crystal is established by TG/DTA. The nonlinear optical studies (SHG) of the crystal have been determined using the Kurtz and Perry powder technique and the activity observed is 2.5 times greater than that of KDP.
 
Publisher IOR PRESS
 
Date 2021-01-05
 
Type info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
Peer-reviewed Article
 
Format application/pdf
 
Identifier https://www.journals.iorpress.org/index.php/bsr/article/view/193
10.34256/bsr2112
 
Source Bulletin of Scientific Research; Vol. 3 No. 1 (2021): Volume 3 Issue 1 Year 2021; 13-20
2582-4678
10.34256/bsr211
 
Language eng
 
Relation https://www.journals.iorpress.org/index.php/bsr/article/view/193/135
 
Rights Copyright (c) 2021 Mohanraj V, Ilango S.S., Ponnuswamy S
https://creativecommons.org/licenses/by/4.0
 

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