COMPARATIVE STUDY ON SYNTHESIS OF METAL ORGANIC FRAMEWORK-199 BY MICROWAVE AND SOLVOLTHERMAL PROCESS

Hue University Journal of Science: Natural Science

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Field Value
 
Title COMPARATIVE STUDY ON SYNTHESIS OF METAL ORGANIC FRAMEWORK-199 BY MICROWAVE AND SOLVOLTHERMAL PROCESS
 
Creator Vinh Thien, Tran
 
Subject Chemistry
MOF-199, comparative, microwave, solvolthermal
 
Description In the present paper, a comparative study on the synthesis of metal organic framework-199 by microwave and solvolthermal method was demonstrated. The obtained materials were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), nitrogen adsorption/desorption isotherms and thermal gravity (TG). The microwave synthesis of MOF-199 has been compared to its conventional hydrothermal synthesis. It is found that by using microwave synthesis MOF-199 can be obtained in a much shorter synthesis time with improved yield and textural properties. It is supposed that the microwave energy emitted fast and uniformly, creating nuclei through the solution which quickly grew to crystals and both the nucleation and crystallization steps were accelerated. These make the microwave synthesis advantages over solvolthermal synthesis.
 
Publisher Hue University
 
Contributor
 
Date 2017-12-29
 
Type info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion



 
Format application/pdf
 
Identifier http://jos.hueuni.edu.vn/index.php/HUJOS-NS/article/view/4455
10.26459/hueuni-jns.v126i1C.4455
 
Source Hue University Journal of Science: Natural Science; Vol 126, No 1C (2017): Hue University Journal of Science: Natural Science; 107-116
Khoa học Tự Nhiên; Vol 126, No 1C (2017): Hue University Journal of Science: Natural Science; 107-116
1859-1388
1859-1388
10.26459/hueuni-jns.v126i1C
 
Language eng
 
Relation http://jos.hueuni.edu.vn/index.php/HUJOS-NS/article/view/4455/366
 
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Rights Copyright (c) 2017 Hue University Journal of Science: Natural Science
 

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